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Herein, a two-step process to synthesize the highly active and robust Pt/TiO2 nanostructures with the engineered surface area is presented. A 3D open-cellular architecture with interconnected micro-nanostructure is first generated by the sol-gel reaction between titanium isopropoxide and tetraethyl orthosilicate (TEOS). After aging in an ammonia solution for 12 h, the TiO2 nanorods decorated with Pt nanoparticles are formed. The samples are characterized by x-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution TEM (HRTEM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), N2 adsorption-desorption, and electrochemical analysis. Results show that the Pt nanoparticles are well-distributed in the nanorod with about 5 nm in diameter and 5 nm in length. The resulting Pt/TiO2 samples exhibit an enhanced surface area, active Pt-oxide species, a narrowed bandgap and enhanced electrochemical activity toward hydrogen evolution reaction (HER). The electrocatalytic activity can be significantly improved by increasing the proportion of Pt in the TiO2 nanostructures.Microsoft may have had a rough 2020 0b46394aab